CHARACTERIZATION AND HAIR DYEING APPLICATION  OF GREEN SYNTHESIS SILVER NANOPARTICLES  USING CRATOXYLUM PRUNIFLORUM (KURZ) KURZ EXTRACT

Lưu Trần Đức Lương; Nguyễn Phú Bình; Lương Văn Luyện; Ngô Tuấn Vinh

doi:10.34238/tnu-jst.12055

CHARACTERIZATION AND HAIR DYEING APPLICATION OF GREEN SYNTHESIS SILVER NANOPARTICLES USING CRATOXYLUM PRUNIFLORUM (KURZ) KURZ EXTRACT

About this article

Received: 14/02/25 Revised: 11/03/25 Published: 11/03/25

Authors

1. Luu Tran Duc Luong, Viet Bac Highlands High School
2. Nguyen Phu Binh, Viet Bac Highlands High School
3. Luong Van Luyen, Viet Bac Highlands High School
4. Ngo Tuan Vinh , Viet Bac Highlands High School

Abstract

This study focuses on the green synthesis of silver nanoparticles (AgNPs) from the leaf extract of Cratoxylum pruniflorum and their application in hair dyeing. The aim is to analyze the physical properties of AgNPs and their potential use in hair dyeing. AgNPs were synthesized through the reduction of Ag⁺ from an AgNO₃ solution using the leaf extract of C. pruniflorum. Several analytical techniques, including UV-Vis spectroscopy, X-ray diffraction, Fourier-transform infrared spectroscopy, transmission electron microscopy, and scanning electron microscopy, were employed to characterize the AgNPs. UV-Vis analysis revealed a characteristic absorption peak at 437 nm, confirming the presence of AgNPs. X-ray diffraction patterns showed a face-centered cubic structure of the nanoparticles. Fourier-transform infrared spectroscopy analysis indicated that functional groups such as O-H, C=O, C-H, and C-O from the extract played a role in the reduction and stabilization of the nanoparticles. Transmission electron microscopy, and scanning electron microscopy images revealed spherical AgNPs with sizes ranging from 5 to 40 nm and a uniform size distribution. The application of the AgNPs solution in hair dyeing resulted in a uniform black color that remained stable even after 20-30 washes. Sensitivity tests on Swiss white mice showed no signs of inflammation or skin irritation, confirming the safety of the product. These findings suggest that silver nanoparticles from C. pruniflorum leaf extract have promising potential for use in safe and effective hair dye products.

Keywords

Cratoxylum pruniflorum; X-ray diffraction; Scanning electron microscopy; Transmission electron microscopy; Silver nanoparticle

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References

[1] K. Khaldoun, S. Khizar, S. Saidi-Besbes, N. Zine, A. Errachid, and A. Elaissari, “Synthesis of silver nanoparticles as an antimicrobial mediator,” J. Umm Al-Qura Univ. Appll. Sci., Jun. 2024, doi: 10.1007/s43994-024-00159-5.

[2] M. Fahim, A. Shahzaib, N. Nishat, A. Jahan, T. A. Bhat, and A. Inam, “Green synthesis of silver nanoparticles: A comprehensive review of methods, influencing factors, and applications,” JCIS Open, vol. 16, Dec. 2024, Art. no. 100125, doi: 10.1016/j.jciso.2024.100125.

[3] P. Ngamsurach and P. Praipipat, “Modified Alginate Beads with Ethanol Extraction of Cratoxylum formosum and Polygonum odoratum for Antibacterial Activities,” ACS Omega, vol. 6, no. 47, pp. 32215–32230, Nov. 2021, doi: 10.1021/acsomega.1c05056.

[4] A. Raksat, S. Laphookhieo, S. Cheenpracha, T. Ritthiwigrom, and W. Maneerat, “Antibacterial Compounds from the Roots of Cratoxylum formosum spp. pruniflorum,” Natural Product Communications, vol. 9, no. 10, Oct. 2014, Art. no. 1934578X1400901020, doi: 10.1177/1934578X1400901020.

[5] M. S. Khalil et al., “Fabrication of Silver Nanoparticles from Ziziphus nummularia Fruit Extract: Effect on Hair Growth Rate and Activity against Selected Bacterial and Fungal Strains,” Journal of Nanomaterials, vol. 2022, no. 1, Jan. 2022, Art. no. 3164951, doi: 10.1155/2022/3164951.

[6] Y. Tang, Z. Zhang, S. Yang, G. J. Smith, and L. Liu, “Diatomite encapsulated AgNPs as novel hair dye cosmetics: Preparation, performance, and toxicity,” Colloids and Surfaces B: Biointerfaces, vol. 200, Apr. 2021, Art. no. 111599, doi: 10.1016/j.colsurfb.2021.111599.

[7] L. He, F. Michailidou, H. L. Gahlon, and W. Zeng, “Hair Dye Ingredients and Potential Health Risks from Exposure to Hair Dyeing,” Chem. Res. Toxicol., vol. 35, no. 6, pp. 901–915, Jun. 2022, doi: 10.1021/acs.chemrestox.1c00427.

[8] C. Battistella, N. C. McCallum, K. Gnanasekaran, X. Zhou, V. Caponetti, M. Montalti, and N. C. Gianneschi, “Mimicking Natural Human Hair Pigmentation with Synthetic Melanin,” ACS Cent. Sci., vol. 6, no. 7, pp. 1179–1188, Jul. 2020, doi: 10.1021/acscentsci.0c00068.

[9] T. T. H. Le, T. H. Ngo, T. H. Nguyen, V. H. Hoang, V. H. Nguyen, and P. H. Nguyen, “Anti-cancer activity of green synthesized silver nanoparticles using Ardisia gigantifolia leaf extract against gastric cancer cells,” Biochemical and Biophysical Research Communications, vol. 661, pp. 99–107, Jun. 2023, doi: 10.1016/j.bbrc.2023.04.037.

[10] S. Jaast and A. Grewal, “Green synthesis of silver nanoparticles, characterization and evaluation of their photocatalytic dye degradation activity,” Current Research in Green and Sustainable Chemistry, vol. 4, 2021, Art. no. 100195, doi: 10.1016/j.crgsc.2021.100195.

[11] I. -M. Chung, I. Park, K. Seung-Hyun, M. Thiruvengadam, and G. Rajakumar, “Plant-Mediated Synthesis of Silver Nanoparticles: Their Characteristic Properties and Therapeutic Applications,” Nanoscale Res Lett, vol. 11, no. 1, Dec. 2016, Art. no. 40, doi: 10.1186/s11671-016-1257-4.

[12] A. G. Femi-Adepoju, A. O. Dada, K. O. Otun, A. O. Adepoju, and O. P. Fatoba, “Green synthesis of silver nanoparticles using terrestrial fern (Gleichenia Pectinata (Willd.) C. Presl.): characterization and antimicrobial studies,” Heliyon, vol. 5, no. 4, Apr. 2019, Art. no. e01543, doi: 10.1016/j.heliyon. 2019.e01543.

[13] P. Wongsa, P. Phatikulrungsun, and S. Prathumthong, “FT-IR characteristics, phenolic profiles and inhibitory potential against digestive enzymes of 25 herbal infusions,” Sci. Rep., vol. 12, no. 1, Apr. 2022, Art. no. 6631, doi: 10.1038/s41598-022-10669-z.

DOI: https://doi.org/10.34238/tnu-jst.12055

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