Email this article FAST AND SIMPLE SYNTHESIS OF FERROMAGNETIC IRON OXIDE NANOPARTICLES BY A PLASMA-SOLUTION INTERACTION METHOD
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Received: 10/07/20 Revised: 30/08/20 Published: 31/08/20Authors
1. Nguyen Van Hao, TNU - University of Science2. Trinh Thi Linh, TNU - University of Science
3. Pham Van Hao, TNU - University of Information and Communication Technology
4. Dang Van Thanh, TNU - University of Medicine and Pharmarcy
5. Do Hoang Tung
, Institute of Physics - Vietnam Academy of Science and Technology
Abstract
This paper presents a simple, fast and environmentally friendly method for preparing Fe3O4 nanoparticles. Fe3O4 nanoparticles are synthesized by plasma-solution interaction at atmospheric pressure using ferrous and ferric solution. The characteristics of Fe3O4 nanoparticles were investigated by X-ray diffraction methods (XRD), transmission electron microscopy (TEM) and vibration sample magnetometer (VSM). Magnetite nanoparticles obtained were spherical in shape with an average size of 11.5 nm and saturation magnetic (Ms) of Fe3O4 sample at room temperature was 52.04 emu/g. Therefore, Fe3O4 nanoparticles are suitable to remove Reactive Red 21 (RR21) pigment in water by a simple magnetic separation process. The RR21 adsorption efficiency of Fe3O4 nanoparticles was achieved up to 75.28%.
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[1]. T. Neuberger, et al., “Superparamagnetic nanoparticles for biomedical applications: possibilities and limitations of a new drug delivery system,” Journal of Magnetism and Magnetic Materials, vol. 293, no. 1, pp. 483-496, 2005.
[2]. K. Onar, and M. E. Yakinci, “Synthesis of Fe3O4 nanoparticles for biomedical applications,” Journal of Physics: Conference Series, vol. 667, p. 012005, 2016.
[3]. S. A. M. K. Ansari, “Eleonora Ficiarà et al., Magnetic Iron Oxide Nanoparticles: Synthesis, Characterization and Functionalization for Biomedical Applications in the Central Nervous System,” Materials, vol. 12, p. 465, 2019.
[4]. A. Zaibudeen, and J. Philip, “Magnetic nanofluid based nonenzymatic sensor for urea detection,” Sensors and Actuators B: Chemical, vol. 255, pp. 720-728, 2018.
[5]. H. Rashid, M. A. Mansoor, B. Haider, R. Nasir, S. B. A. Hamid, and A. Abdulrahman, “Synthesis and characterization of magnetite nano particles with high selectivity using in-situ precipitation method,” Separation Science and Technology, vol. 55, no. 6, pp. 1207-1215, 2020.
[6]. W. Wu, C. Jiang, and V. A. Roy, “Recent progress in magnetic iron oxide–semiconductor composite nanomaterials as promising photocatalysts,” Nanoscale, vol. 7, no. 1, pp. 38-58, 2015.
[7]. L. C. Gonçalves, A. B. Seabra, M. T. Pelegrino, D. R. de Araujo, J. S. Bernardes, and P. S. Haddad, “Superparamagnetic Iron Oxide Nanoparticles Dispersed in Pluronic F127 Hydrogel: Potential Uses in Topical Applications,” RSC Advances, vol. 7, pp. 14496-14503, 2017.
[8]. I. Jönkkäri, M. Sorvali, H. Huhtinen, E. Sarlin, T. Salminen, J. Haapanen, J. M. Mäkelä, and J. Vuorinen, “Characterization of Bidisperse Magnetorheological Fluids Utilizing Maghemite (γ-Fe2O3) Nanoparticles Synthetized by Flame Spray Pyrolysis,” Smart Materials and Structures, vol. 26, no. 9, p. 095004, 2017.
[9]. M. Unni, A. M. Uhl, S. Savliwala, B. H. Savitzky, R. Dhavalikar, N. Garraud, D. P. Arnold, L. F. Kourkoutis, J. S. Andrew, and C. Rinaldi, “Thermal Decomposition Synthesis of Iron Oxide Nanoparticles with Diminished Magnetic Dead Layer by Controlled Addition of Oxygen,” ACS Nano, vol. 11, no. 2, pp. 2284-2303, 2017.
[10]. N. Pérez, C. Moya, P. Tartaj, A. Labarta, and X. Batlle, “Aggregation State and Magnetic Properties of Magnetite Nanoparticles Controlled by an Optimized Silica Coating,” Journal of Applied Physics, vol. 121, p. 044304, 2017.
[11]. D. Vivekanand, and K. Vivekanand, “Synthesis and Characterization of Magnetite by Coprecipitation and Sintering and its Characterization,” Materials and Manufacturing Processes, vol. 33, no. 8, pp. 1-5, 2017.
[12]. A. D. Jawwad, Z. Jingyi, M. M. Neel, and W. Xiaole, “Continuous Hydrothermal Synthesis of Inorganic Nanoparticles: Applications and Future Directions,” Chemical Reviews, vol. 117, no. 17, pp. 11125-11238, 2017.
[13]. E. M. Koushika, G. Shanmugavelayutham, P. Saravanan, and C. Balasubramanian, “Rapid synthesis of nano-magnetite by thermal plasma route and its magnetic propertiesm,” Materials and Manufacturing Processes, vol. 33, pp. 1701-1707, 2018.
[14]. H. T. Do, T. T. Tran, and D. C. Nguyen, “Facile synthesis of carbon quantum dots by plasma-liquidinteraction method,” Communications in Physics, vol. 27, no. 4, pp. 311-316, 2017.
[15]. L. Sarma, T. Sarmah, N. Aomoa, S. Sarma, U. Deshpande, H. Bhuyan, S. Ojha, U. Bora, and M. Kakati, “Size-controlled synthesis of superparamagnetic iron-oxide and iron-oxide/iron/carbon nanotube nanocomposites by supersonic plasma expansion technique,” Journal of Physics D: Applied Physics, vol. 51, no. 19, p. 195003, 2018.
[16]. F. Yu, M. Liu, C. Ma, L. Di, B. Dai, and L. Zhang, “A Review on the Promising Plasma-Assisted Preparation of Electrocatalysts,” Nanomaterials, vol. 9, p. 1436, 2019.
[17]. K. S. Kim, and T. H. Kim, “Nanofabrication by thermal plasma jets: From nanoparticles to low-dimensional nanomaterials,” Journal of Applied Physics, vol. 125, p. 070901, 2019.
[18]. V. Hao Nguyen, H. T. Huu, V. Q. Nguyen, X. V. Dam, L. P. Hoang, and L. T. Ha, “Magnetic Fe3O4 Nanoparticle Biochar Derived from Pomelo Peel for Reactive Red 21 Adsorption from Aqueous Solution,” Journal of chemistry, vol. 2020, pp. 1-14, 2020, ID 3080612.
[19]. R. Wang, S. Zuo, W. Zhu, J. Zhang, and J. Fang, “Rapid Synthesis of Aqueous-Phase Magnetite Nanoparticles by Atmospheric Pressure Non-Thermal Microplasma and their Application in Magnetic Resonance Imaging,” Plasma Processes and Polymers, vol. 11, pp. 448-454, 2014.
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